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Chemical shrinkage in thermosetting polymers drives residual stress development and induces residual deformation in composite materials. Accurate characterization of chemical shrinkage during curing is therefore vital to minimize residual stresses through process modeling and optimize composite performance. This work introduces a novel methodology to measure the pre- and post-gelation chemical shrinkage of an epoxy resin using three-dimensional digital image correlation (3D-DIC). Differential scanning calorimetry (DSC) is employed to calculate reaction kinetics and correlate chemical shrinkage with the degree of cure. Rheology experiments are conducted to quantify gelation and validate post-gelation. 3D-DIC post-gelation results show excellent agreement with rheology. Pre-gelation results show the effect of the in-situ curing in the proximity of constraints on the global strain behavior. This work introduced an innovative approach to characterize the chemical shrinkage of thermosets during curing, which will enable accurate residual stress prediction for enhancing thermoset composite performance and provide insight into the in-situ polymer behavior during processing. 

Stereovision systems can extract full-field three-dimensional (3D) displacements of structures by processing the images collected with two synchronized cameras. To obtain accurate measurements, the cameras must be calibrated to account for lens distortion (i.e., intrinsic parameters) and compute the cameras’ relative position and orientation (i.e., extrinsic parameters). Traditionally, calibration is performed by taking photos of a calibration object (e.g., a checkerboard) with the two cameras. Because the calibration object must be similar in size to the targeted structure, measurements on large-scale structures are highly impractical. This research proposes a multi-sensor board with three inertial measurement units and a laser distance meter to compute the extrinsic parameters of a stereovision system and streamline the calibration procedure. In this paper, the performances of the proposed sensor-based calibration are compared with the accuracy of the traditional image-based calibration procedure. Laboratory experiments show that cameras calibrated with the multi-sensor board measure displacements with 95% accuracy compared to displacements obtained from cameras calibrated with the traditional procedure. The results of this study indicate that the sensor-based approach can increase the applicability of 3D digital image correlation measurements to large-scale structures while reducing the time and complexity of the calibration. 

Three-dimensional digital image correlation (3D-DIC) has become a strong alternative to traditional contact-based techniques for structural health monitoring. 3D-DIC can extract the full-field displacement of a structure from a set of synchronized stereo images. Before performing 3D-DIC, a complex calibration process must be completed to obtain the stereovision system’s extrinsic parameters (i.e., cameras’ distance and orientation). The time required for the calibration depends on the dimensions of the targeted structure. For example, for large-scale structures, the calibration may take several hours. Furthermore, every time the cameras’ position changes, a new calibration is required to recalculate the extrinsic parameters. The approach proposed in this research allows determining the 3D-DIC extrinsic parameters using the data measured with commercially available sensors. The system utilizes three Inertial Measurement Units with a laser distance meter to compute the relative orientation and distance between the cameras. In this paper, an evaluation of the sensitivity of the newly developed sensor suite is provided by assessing the errors in the measurement of the extrinsic parameters. Analytical simulations performed on a 7.5 x 5.7 m field of view using the data retrieved from the sensors show that the proposed approach provides an accuracy of ~10-6 m and a promising way to reduce the complexity of 3D-DIC calibration.